P G Diploma in Analytical Techniques

Potentiometry 1. Halide Estimation 2. Solubility of sparingly soluble salts 3. Dissociation constant of acid Conductometry : 1. Acid-Base titration 2. Effect of concentration on equivalent conductance of a given electrolyte pH metry 1. Acid-Base titration Polarography 1. Detennination of half-wave potential 2. Estimation of Zn2+ ions Radioactivity 1. Detennination of half-life of a radioactive isotope 2. Measurement of thickness of the sample using radiation gauge 3. Elemental analysis of industrial alloys by neutron activation analysis 4. Counting errors UV-visible spectroscopy 1. Determination of molar composition of complex 2. Determination of indicator constant of an indicator. Water Analysis 1.Determination of physico-chemical parameters of water Purification and separation techniques 1.Purification of aniline by distillation method 2.Crystallization of various compounds and their TLC study 3.Column chromatographic method for separation of compounds Food and body fluid analysis 1. Estimation of free fatty acid in oil 2. Determination of serum cholesterol 3. Estimation of reducing sugar 4. Estimation of amino acid by Ninhydrin method 5. Estimation of protein by Lowry method PGB 5 Practical Course 2 (5 credits) Part A : Industrial visits and in plant training for 3 weeks Part B : Demonstration practical based on following techniques 1. HPLC 2. GCMS 3. NMR 4. FTIR 5. XRD 6. TGA 7. AAS 8. SEM Part C : Seminars References 1. Instrumental methods of analysis H.H.Wilard,L.L.Merritt, J A Dean. 2 Instrumental Methods of Chemical analysis. 3 Analytical Chemistry G.D. Chritiain. Wiley 4 Introduction of instrumental analysis. R.P.Braun 5 Essentials of Nuclear Chemistry- H.J.Arnikar 6 A text book of quantitative Inorganic analysis A I Vogel. 7 Pharmo copie of India Britiesh Pharma copoeia 8 Standard methods of Chemical analysis A Series of Volutms Edited F.J.Welcher R.G. Krieger publ-Company. 9 Principles of Instrumental Analysis Fifth edition Skoog, Holler, Niemay.